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Sample Weight: 0.2 g

Summary

Sixteen major, minor, and trace elements are determined in geological materials using a lithium metaborate fusion with an Inductively Coupled Plasma-Optical Emission Spectroscopy (ICP-OES) finish. The sample is fused with lithium metaborate and dissolved using dilute HNO3 in a graphite crucible. The resulting solution is analyzed by Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES).

Method 16 Elements and Reporting Limits
Element Concentration (low) Concentration (high)
Aluminum, Al .005% 75%
Barium, Ba .005% 10%
Calcium, Ca .005% 60%
Chromium, Cr .005% 10%
Iron, Fe .005% 75%
Magnesium, Mg .005% 30%
Manganese, Mn .005% 10%
Niobium, Nb .001% 10%
Phosphorous, P .005% 25%
Potassium, K .005% 25%
Silicon, Si .005% 90%
Sodium, Na .005% 30%
Strontium, Sr .005% 10%
Titanium, Ti .005% 25%
Yttrium, Y .001% 10%
Zirconium, Zr .001% 10%
LOI 0.01% 50%

Analytical Performance

Data will be deemed acceptable if recovery of each element is ±15% at five times the Lower Limit of Determination (LOD) and the calculated Relative Standard Deviation (RSD) of duplicate samples is no greater than 15%.

Project Contact

Jaime Azain
Phone: 303-236-9376
Email: jsazain@usgs.gov
Central Mineral and Environmental Resources Science Center

Mineral Resources Program Science Priority

The use of firm, trade, and brand names is for identification purposes only and does not constitute endorsement by the U.S. government.

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